Page 1. SYNTHETIC COMMUNICATIONS, 18(3), 227-232 (1988) A FACILE SYNTHESIS OF UNSYMMETRICAL THIOLSULFONATES VIA SULFONYLATION OF MERCAPTANS1 MG Ranasinghe, PL Fuchs· Department of Chemistry Purdue University west Lafayette, IN 47907 Abstract: The reaction of p-toluenesulfonyl bromide with mercaptans provides a convenient procedure for the synthesis of unsymmetrical thiolsulfonates. ...