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The Journal of Organic Chemistry

Synthesis of bridgehead-substituted bicyclo [2.2. 1] heptanes by radical cyclization

EW Della, AM Knill, PE Pigou

文献索引：Della, Ernest W.; Knill, Andrew M.; Pigou, Paul E. Journal of Organic Chemistry, 1993 , vol. 58, # 8 p. 2110 - 2114

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被引用次数: 8

摘要

ylenecyclohexane (161, both of which were identified by comparison with authentic specimens. This result was encouraging from the point of view of ita synthetic potential, it also provides qualitative confirmation of the conclusions reached by the force-field calculations, viz., that the isomerization 3-4 does have a significant energy barrier. A quantitative estimate of the activation energy temp, OC

1-[(Tosyloxy)methyl]-4-methylenecyclohexane结构式

1-[(Tosyloxy)me...

~73%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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尼泊金乙酯结构式

尼泊金乙酯

~%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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(4-亚甲基环已基)甲醇结构式

(4-亚甲基环已基)甲醇

~%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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反-4-羟基环己烷甲酸乙酯结构式

反-4-羟基环己烷甲酸乙酯

~%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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4-氧代环己甲酸乙酯结构式

4-氧代环己甲酸乙酯

~%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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4-亚甲基环己烷-1-甲酸乙酯结构式

4-亚甲基环己烷-1-甲酸乙酯

~%

1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

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尼泊金乙酯结构式

尼泊金乙酯

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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反-4-羟基环己烷甲酸乙酯结构式

反-4-羟基环己烷甲酸乙酯

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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(4-亚甲基环已基)甲醇结构式

(4-亚甲基环已基)甲醇

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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4-氧代环己甲酸乙酯结构式

4-氧代环己甲酸乙酯

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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4-亚甲基环己烷-1-甲酸乙酯结构式

4-亚甲基环己烷-1-甲酸乙酯

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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1-[(Tosyloxy)methyl]-4-methylenecyclohexane结构式

1-[(Tosyloxy)me...

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

~%

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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1-(Hydroxymethyl)bicyclo(2.2.1)heptane结构式

1-(Hydroxymethy...

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

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二环[2.2.1]庚烷-1-羧酸结构式

二环[2.2.1]庚烷-1-羧酸

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

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bicyclo(2.2.1)heptan-1-ylmethyl toluene-p-sulphonate结构式

bicyclo(2.2.1)h...

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

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4-(bromomethyl)bicyclo[2.2.1]heptane结构式

4-(bromomethyl)...

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

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1-(Bromomethyl)-4-methylidenecyclohexane结构式

1-(Bromomethyl)...

~%

4-methylbicyclo[2.2.1]heptane结构式

4-methylbicyclo...

1-Methyl-4-methylenecyclohexane.结构式

1-Methyl-4-meth...

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bicyclo(2.2.1)heptan-1-ylmethyl toluene-p-sulphonate结构式

bicyclo(2.2.1)h...

~85%

4-(bromomethyl)bicyclo[2.2.1]heptane结构式

4-(bromomethyl)...

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1-(Hydroxymethyl)bicyclo(2.2.1)heptane结构式

1-(Hydroxymethy...

~%

4-(bromomethyl)bicyclo[2.2.1]heptane结构式

4-(bromomethyl)...

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二环[2.2.1]庚烷-1-羧酸结构式

二环[2.2.1]庚烷-1-羧酸

~%

4-(bromomethyl)bicyclo[2.2.1]heptane结构式

4-(bromomethyl)...

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