Enantiomeric quantifications of amino acids through their Na??Acyl amides by gas chromatography

N Hosten, MJO Anteunis

文献索引：Hosten, N.; Anteunis, M. J. O. Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 1 p. 45 - 47

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被引用次数: 4

摘要

Abstract Apparent separation factors of 1.1 or higher on Chirasil Val III can be obtained for N a-acyl N-alkyl aminoacid amides allowing the use of short capillary gas chromatographic columns. A clean derivatization protocol without racemization is described, proceding through the NCA derivatives that are prepared from “in situ” silylated amino acids with trimethylsilyl cyanide.