Synthesis, NMR Studies and Crystal Structure of Cryptand 4, 7, 10, 16, 21-Pentaoxa-1, 13-diazabicyclo [11.5. 5] tricosane,[H (3.1. 1)·(H2O) 3] Cl

T Nguyen, CM Buckley, TK Ellis, GLN Smith…

文献索引：Nguyen, Tam; Buckley, Christopher M.; Ellis, Trevor K.; Smith, Gary L. N.; Powell, Douglas R.; Taylor, Richard W. Journal of Chemical Crystallography, 2012 , vol. 42, # 6 p. 573 - 577

全文：HTML全文

被引用次数: 0

摘要

Abstract The cryptand 4, 7, 10, 16, 21-pentaoxa-1, 13-diazabicyclo 11.5. 5 tricosane (3.1. 1, I) has been synthesized, the crystal structure of the triaquo-hydrochloride salt has been determined by single crystal X-ray crystallography and the 1 H-and 13 C-NMR chemical shifts have been assigned for the protonated ligand.(C 16 H 33 N 2 O 5)·(H 2 O) 3 Cl,(I), is triclinic with space group P ̄ 1 and cell constants: a= 9.957 (3) Å, b= 10.557 (5) Å, c= ...