Abstract: A simple homologous series of 3-[4-alkyloxyphenyl]-5-[3, 4-methylenedioxybenzyl]- 2-isoxazolines having chiral sources have been synthesized by the reaction of nitrile oxides isolated from the dehydrogenation of 4-alkyloxyphenyl aldoximes using chloramine-T with safrole. Synthesized compounds structures have been confirmed by 1 H NMR, 13 C NMR, mass spectral analysis and optical texture studies have been carried out using Leitz ...