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举例 :可输入Filippa Pettersson 或者 Cancer Res. 75(6) , 1102-12, (2015) 或者10.1002/anie.201600521

Synthesis

Synthesis of 2, 3-Dihydro-1, 4-dithiins and 2-Alkylidene-1, 4-dithianes by 1, 2-Sulfur Migration in 2-(1-Hydroxyalkyl)-1, 3-dithiolanes

CAM Afonso, MT Barros, LS Godinho, CD Maycock

文献索引：Afonso; Barros; Godinho; Maycock Synthesis, 1991 , # 7 p. 575 - 580

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被引用次数: 17

摘要

Product Yield Ratio 3+ 4 (V0) 3/4 Sub-Ratio 2/Temp. Time strate Et2O~ BF3 (C)(h) la 1.0 25 12 3a 92-111 0.7 25 2 3h 57-lc 1.0 0 2 3c 38-1d 0.8 0 2 3d 97-le 0.8 25 12 3e 90-If 0.8 25 2 3r+ 4r 95 1.5 lg 0.8 25 2 3g+ 4g 96 1.3 lb 0.8 0 2 an+ 411 90 0.59 li 1.0 0 2 3i+ 4i 56 0.18 Si 1.0 0 2 41 74 0 5j 1.0 0 1 41 75 0

1,2-乙二硫醇结构式

1,2-乙二硫醇

1-苯基-1,2-丙二酮结构式

1-苯基-1,2-丙二酮

~%

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1-(2-phenyl-1,3-dithiolan-2-yl)ethanone结构式

1-(2-phenyl-1,3...

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Ethanone, 1-(2-methyl-1,3-dithiolan-2-yl)- (9CI)结构式

Ethanone, 1-(2-...

~%

2,3-dihydro-5,6-dimethyl-1,4-dithiin结构式

2,3-dihydro-5,6...

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1-(2-methyl-1,3-dithiolan-2-yl)ethan-1-ol结构式

1-(2-methyl-1,3...

~93%

2,3-dihydro-5,6-dimethyl-1,4-dithiin结构式

2,3-dihydro-5,6...

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1-(2-phenyl-1,3-dithiolan-2-yl)ethanol结构式

1-(2-phenyl-1,3...

~96%

5-methyl-6-phenyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-6-phen...

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(2-methyl-1,3-dithiolan-2-yl)(phenyl)methanol结构式

(2-methyl-1,3-d...

~75%

5-methyl-6-phenyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-6-phen...

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1-苯基-1,2-丙二酮结构式

1-苯基-1,2-丙二酮

~%

5-methyl-6-phenyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-6-phen...

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未登录结构式

~%

5-methyl-6-phenyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-6-phen...

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1-(2-phenyl-1,3-dithiolan-2-yl)ethanone结构式

1-(2-phenyl-1,3...

~%

5-methyl-6-phenyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-6-phen...

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(2-methyl-1,3-dithiolan-2-yl)methanol结构式

(2-methyl-1,3-d...

~97%

5-methyl-2,3-dihydro-1,4-dithiine结构式

5-methyl-2,3-di...

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1-(2-ethyl-1,3-dithiolan-2-yl)propan-1-ol结构式

1-(2-ethyl-1,3-...

~24%

5,6-diethyl-2,3-dihydro-1,4-dithiine结构式

5,6-diethyl-2,3...

2-ethyl-3-ethylidene-1,4-dithiane结构式

2-ethyl-3-ethyl...

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3,4-己二酮结构式

~%

5,6-diethyl-2,3-dihydro-1,4-dithiine结构式

5,6-diethyl-2,3...

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1-(2-ethyl-1,3-dithiolan-2-yl)propan-1-one结构式

1-(2-ethyl-1,3-...

~%

5,6-diethyl-2,3-dihydro-1,4-dithiine结构式

5,6-diethyl-2,3...

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1-(2-ethyl-1,3-dithiolan-2-yl)propan-1-ol结构式

1-(2-ethyl-1,3-...

~%

5,6-diethyl-2,3-dihydro-1,4-dithiine结构式

5,6-diethyl-2,3...

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2-ethyl-3-ethylidene-1,4-dithiane结构式

2-ethyl-3-ethyl...

~%

5,6-diethyl-2,3-dihydro-1,4-dithiine结构式

5,6-diethyl-2,3...

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