前往化源商城

Journal of the American Chemical Society

PHOTOCHEMICAL REACTIONS OF METHYL DIAZOACETATE WITH POLYHALOMETHANES

WH Urry, JW Wilt

文献索引:Urry; Wilt Journal of the American Chemical Society, 1954 , vol. 76, p. 2594

全文:HTML全文

被引用次数: 21

摘要

(1) WH Urrp and JR Eiszner, THIS JOURNAL, 74, 5822 (1952). over a period of eight hours. Products identified after distillation were methyl chloroacetate (5.55 g., 0.051 mole, bp 47- 52'at 18 mm.,%* OD 1.4660, mol. wt. Rast, 106, gave N-phenylglycine, mp 12702 when treated by the method of Koelsch3 in an attempt to form the anilide), and presumed methyl a, P, P-trichloropropionate (2.35 g., 0.02 mole, bp 85-90'at 18 mm., nZo~ 1.4626, mol. wt. ...