Page 1. SYNTHETIC COMMUNICATIONS, 1 7 ( 4 ) , 457-464 (1987) CARBOXYLATION OF ARENES ... To the organic phase was then added an equal volume of water and the whole distilled until all the ... mp lit.' 87.5OC 1-(4-Methylphenyl)-2,2,2-trichloroethanol(lb) (88%) , ...