α-Thiocyanation of carbonyl and β-dicarbonyl compounds using (dichloroiodo) benzene-lead (II) thiocyanate

…, H Batra, N Rani, SP Singh, RM Moriarty

文献索引：Prakash; Kaur; Batra; Rani; Singh; Moriarty Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 2019 - 2023

被引用次数: 65

摘要

The combination reagent (dichloroiodo) benzene and lead (II) thiocyanate in dichloromethane effects oxidation of various enol silyl ethers, ketene silyl acetals, and β- dicarbonyl compounds, thereby providing an efficient and convenient method for α- thiocyanation of carbonyl and β-dicarbonyl compounds.

13735-81-4

1-苯基-1-三甲基硅氧乙烯

~61%

~92%

~46%

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