The Journal of Organic Chemistry

Synthesis and Reactions of 1-Nitroso-1-alkyl-2-guanyl-and-2-carbamylhydrazines

WG Finnegan, RA Henry

文献索引：Finnegan,W.G.; Henry,R.A. Journal of Organic Chemistry, 1965 , vol. 30, p. 567 - 575

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被引用次数: 11

摘要

568 FINNEQAN AND HENRY VOL. 30 chloride. The decomposition of l-benzyl-2-guanyl- lnitrosohydrazine (11) in concentxat'ed hydrochloric acid at ambient temperature for 2-4 hr. or at steambat'h temperature for a few minutes (until the exothermic reaction subsided) led to the formation of benzyl chloride, ammonium chloride, and carbamyl azide in good yields. A similar decomposition, run in ghcial acetic acid at 100'for 5 min., yielded benzyl acetate, a ...