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举例 :可输入Filippa Pettersson 或者 Cancer Res. 75(6) , 1102-12, (2015) 或者10.1002/anie.201600521

A Scalable Process to the Key Intermediate of Cilazapril,(S)-1-Benzyloxycarbonylhexahydropyridazine-3-carboxylic Acid, Through a Novel Cascade Course

Y Chen, Y Lu, Q Zou, H Chen, D Ma

文献索引：Attwood, Michael R.; Hassall, Cedric H.; Kroehn, Antonin; Lawton, Geoffrey; Redshaw, Sally Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1011 - 1020

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被引用次数: 4

摘要

... Dev. All Publications/Website. Select a Journal or Book ... Process Res. Dev. , 2013, 17 (9), pp 1209–1213. DOI: 10.1021/op400155u. Publication Date (Web): July 29, 2013. Copyright © 2013 American Chemical Society. ... entry, 4 (equiv), solvent, temp (°C), time (h), yield of 5 (%) b. ...

TERT-BUTYL (1S,9S)-6,10-DIOXO-9-PHTHALIMIDOOCTAHYDROPYRIDAZO[1,2-A][1,2]DIAZEPINE-1-CARBOXYLATE结构式

TERT-BUTYL (1S,...

~90%

(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯结构式

(1S,9S)-9-(1,3-...

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2(S)-4-Benzoyloxy carbonyl-2-phthalimido butyryl chloride结构式

2(S)-4-Benzoylo...

~%

(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯结构式

(1S,9S)-9-(1,3-...

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未登录结构式

~%

(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯结构式

(1S,9S)-9-(1,3-...

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(S)-1-benzyl-3-tert-butyl piperazine-1,3-dicarboxylate结构式

(S)-1-benzyl-3-...

~%

(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯结构式

(1S,9S)-9-(1,3-...

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(S)-5-(苄氧基)-2-(1,3-二氧代异吲哚啉-2-基)-5-氧代戊酸结构式

(S)-5-(苄氧基)-2-(...

~%

(1S,9S)-9-(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)八氢-10-氧代-6H-哒嗪并[1,2-A][1,2]二氮杂卓-1-羧酸叔丁酯结构式

(1S,9S)-9-(1,3-...

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2(S)-4-Benzoyloxy carbonyl-2-phthalimido butyryl chloride结构式

2(S)-4-Benzoylo...

~%

TERT-BUTYL (1S,9S)-6,10-DIOXO-9-PHTHALIMIDOOCTAHYDROPYRIDAZO[1,2-A][1,2]DIAZEPINE-1-CARBOXYLATE结构式

TERT-BUTYL (1S,...

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未登录结构式

~%

TERT-BUTYL (1S,9S)-6,10-DIOXO-9-PHTHALIMIDOOCTAHYDROPYRIDAZO[1,2-A][1,2]DIAZEPINE-1-CARBOXYLATE结构式

TERT-BUTYL (1S,...

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(S)-1-benzyl-3-tert-butyl piperazine-1,3-dicarboxylate结构式

(S)-1-benzyl-3-...

~%

TERT-BUTYL (1S,9S)-6,10-DIOXO-9-PHTHALIMIDOOCTAHYDROPYRIDAZO[1,2-A][1,2]DIAZEPINE-1-CARBOXYLATE结构式

TERT-BUTYL (1S,...

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(S)-5-(苄氧基)-2-(1,3-二氧代异吲哚啉-2-基)-5-氧代戊酸结构式

(S)-5-(苄氧基)-2-(...

~%

TERT-BUTYL (1S,9S)-6,10-DIOXO-9-PHTHALIMIDOOCTAHYDROPYRIDAZO[1,2-A][1,2]DIAZEPINE-1-CARBOXYLATE结构式

TERT-BUTYL (1S,...

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2(S)-4-Benzoyloxy carbonyl-2-phthalimido butyryl chloride结构式

2(S)-4-Benzoylo...

~%

1-(S)-顺式-9-氨基八氢-10-氧代-6H-吡嗪并[1,2-a][1,2]二氮杂卓-1-羧酸叔丁酯结构式

1-(S)-顺式-9-氨基八氢...

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未登录结构式

~%

1-(S)-顺式-9-氨基八氢-10-氧代-6H-吡嗪并[1,2-a][1,2]二氮杂卓-1-羧酸叔丁酯结构式

1-(S)-顺式-9-氨基八氢...

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(S)-1-benzyl-3-tert-butyl piperazine-1,3-dicarboxylate结构式

(S)-1-benzyl-3-...

~%

1-(S)-顺式-9-氨基八氢-10-氧代-6H-吡嗪并[1,2-a][1,2]二氮杂卓-1-羧酸叔丁酯结构式

1-(S)-顺式-9-氨基八氢...

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(S)-5-(苄氧基)-2-(1,3-二氧代异吲哚啉-2-基)-5-氧代戊酸结构式

(S)-5-(苄氧基)-2-(...

~%

1-(S)-顺式-9-氨基八氢-10-氧代-6H-吡嗪并[1,2-a][1,2]二氮杂卓-1-羧酸叔丁酯结构式

1-(S)-顺式-9-氨基八氢...

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(1S,9S)-t-butyl 9-((1S)-ethoxycarbonyl-3-phenylpropylamino)octahydro-10-oxo-6H-pyridazino(1,2-a)(1,2)diazepine-1-carboxylate结构式

(1S,9S)-t-butyl...

~91%

西拉普利结构式

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