Organic Process Research & Development

A Large, Laboratory-Scale Synthesis of [4-(2-(2 H)-Tetrahydropyranyloxy) phenyl] boronic Acid

DE Cladingboel

文献索引：Organic Process Research and Development, , vol. 4, # 3 p. 153 - 155

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被引用次数: 30

摘要

... Organic Process Research & Development. ... Efficient cooling is essential during the crystallisation due to the exothermic nature of the process, and, if allowed to ... The mixture was stirred vigorously for 1 h before the organic phase was separated, dried over anhydrous magnesium ...