Safety Assessment for the Scale-up of an Oxime Reduction with Melted Sodium in Standard Pilot-Plant Equipment

RA Breitenmoser, T Fink, S Abele

文献索引：Kawada, Kenji; Tsushima, Tadahiko Heterocycles, 1989 , vol. 28, # 2 p. 573 - 578

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摘要

... However, the high dilution would result in a very low volume throughput. ... Table 2. Familiarization runs using cyclohexanone oxime 4 as model substrate a. ... 1 c, 4M2P 6 equiv, 10.5 vol, dose 4 in 4 equiv 4M2P to Na in xylenes at 105 °C; dose 2 equiv 4M2P, 0. ...