Tetrahedron letters

5, 6-dihydropyridine: synthesis and characterization

MC Lasne, JL Ripoll, JC Guillemin, JM Denis

文献索引：Lasne, Marie-Claire; Ripoll, Jean-Louis; Guillemin, Jean-Claude; Denis, Jean-Marc Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3847 - 3848

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被引用次数: 10

摘要

Abstract 5, 6-dihydropyridine 1 is synthesized either by flash vacuum thermolysis of 1- azabicyclo [2.2. 2] oct-2-ene 3 or by dehydrochlorination over solid bases of N-chloro-1, 2, 5, 6-tetrahydropyridine 4 and characterized at low temperature by its 1 H and 13 C nmr and ir spectra.