前往化源商城

The Journal of Organic Chemistry

Diphthalimido carbonate: A new reagent for active ester synthesis

K Kurita, H Imajo

文献索引:Kurita, Keisuke; Imajo, Hidetomo Journal of Organic Chemistry, 1982 , vol. 47, # 23 p. 4584 - 4586

全文:HTML全文

被引用次数: 7

摘要

DPC easily purified by recrystallization from ethyl acetate to give colorless granular crystals. DPC is a stable compound and can be kept at room temperature over a long period. It begins to decompose at 153" C in thermogravimetry in air (5 OC/min) without showing a clear melting point. Before the reaction with amino acids, DPC was subjected to the reaction with benzoic and acetic acids in order to establish the general reactivity of the carbonate. ...