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举例 :可输入Filippa Pettersson 或者 Cancer Res. 75(6) , 1102-12, (2015) 或者10.1002/anie.201600521

Reactions of 11-chloro-11-phenyl-6, 11-dihydrodibenzo [b, e]-thiepin with piperidine and some further nucleophiles

M Protiva, K Šindelář, V Valenta…

文献索引：Protiva; Sindelar; Valenta; et al. Collection of Czechoslovak Chemical Communications, 1982 , vol. 47, # 11 p. 3094 - 3113

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被引用次数: 5

摘要

Abstract The title compound Vb affords with piperidine normal nucleophilic substitution product and the isomeric 3-piperidino derivative XXXII. The structure of XXXII was proven by (1) the 1 H NMR and 13 C NMR spectra,(2) an independent synthesis via the intermediates XXXV, XXXVI, XXX, IV and VIIIa, and (3) with the help of model reactions of the 2-methyl derivative VIb and the 3-methyl derivative VIIb with piperidine. The rearranged cation ...

1,5-二溴戊烷结构式

1,5-二溴戊烷

3-溴苯胺结构式

~70%

1-(3-溴苯基)哌啶结构式

1-(3-溴苯基)哌啶

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11-Phenyl-3-piperidino-6,11-dihydrodibenzo[b,e]thiepin-11-ol结构式

11-Phenyl-3-pip...

~50%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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苯酞结构式

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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1,5-二溴戊烷结构式

1,5-二溴戊烷

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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溴苯结构式

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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1-(3-溴苯基)哌啶结构式

1-(3-溴苯基)哌啶

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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3-Piperidinothiophenol结构式

3-Piperidinothi...

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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3-Piperidinodibenzo[b,e]thiepin-11(6H)-one结构式

3-Piperidinodib...

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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2-(3-Piperidinophenylthiomethyl)benzoic Acid结构式

2-(3-Piperidino...

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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11-Phenyl-6,11-dihydrodibenzo(b,e)thiepin-11-ol结构式

11-Phenyl-6,11-...

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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3-溴苯胺结构式

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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6,11-二氢二苯并[b,e]硫杂卓-11-酮结构式

6,11-二氢二苯并[b,e]...

~%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

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六氢吡啶结构式

11-chloro-11-phenyl-6,11-dihydro-dibenzo[b,e]thiepine结构式

11-chloro-11-ph...

~19%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

1-(11-phenyl-6H-benzo[c][1]benzothiepin-11-yl)piperidine结构式

1-(11-phenyl-6H...

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溴苯结构式

~%

1-(11-phenyl-6H-benzo[c][1]benzothiepin-11-yl)piperidine结构式

1-(11-phenyl-6H...

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11-Phenyl-6,11-dihydrodibenzo(b,e)thiepin-11-ol结构式

11-Phenyl-6,11-...

~%

1-(11-phenyl-6H-benzo[c][1]benzothiepin-11-yl)piperidine结构式

1-(11-phenyl-6H...

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6,11-二氢二苯并[b,e]硫杂卓-11-酮结构式

6,11-二氢二苯并[b,e]...

~%

1-(11-phenyl-6H-benzo[c][1]benzothiepin-11-yl)piperidine结构式

1-(11-phenyl-6H...

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六氢吡啶结构式

11-chloro-11-phenyl-6,11-dihydro-dibenzo[b,e]thiepine结构式

11-chloro-11-ph...

~18%

11-Phenyl-3-piperidino-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Phenyl-3-pip...

1-(11-phenyl-6H-benzo[c][1]benzothiepin-11-yl)piperidine结构式

1-(11-phenyl-6H...

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吗啉结构式

11-chloro-11-phenyl-6,11-dihydro-dibenzo[b,e]thiepine结构式

11-chloro-11-ph...

~56%

11-Morpholino-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Morpholino-1...

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溴苯结构式

~%

11-Morpholino-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Morpholino-1...

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11-Phenyl-6,11-dihydrodibenzo(b,e)thiepin-11-ol结构式

11-Phenyl-6,11-...

~%

11-Morpholino-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Morpholino-1...

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6,11-二氢二苯并[b,e]硫杂卓-11-酮结构式

6,11-二氢二苯并[b,e]...

~%

11-Morpholino-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin结构式

11-Morpholino-1...

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