1, 3-Bis (N-methylcarbamoyloxy) benzene (II) was prepared from resorcinol and methyl isocyanate in the same way. The reaction was finish sed after six hours boiling, yield 75%. The product was recrystallized from benzene until constant melting point 154-155 C. For CloH12Nz04 (224'1) found: 53'79% C, 5'63% H, 12'82% N.