Molecular and Supramolecular Structures of 1??Phenyl??4??phenylacetyl??2??thiosemicarbazide (H2L) and its Complexes with Diphenyllead (IV) Chloride and Acetate
Abstract Reaction of 1-phenyl-4-phenylacetyl-2-thiosemicarbazide (H 2 L) with diphenyllead (IV) dichloride and acetate afforded the complexes [PbPh 2 Cl 2 (H 2 L) 2] and [PbPh 2 L]. The ligand and the complexes were characterized by elemental analyses, 1 H and 13 C NMR spectroscopy and X-ray crystallography. In the asymmetric unit of crystals of the ligand there are four independent molecules of H 2 L and four molecules of water, which ...
