New general synthesis for polylithium organic compounds

JR Baran Jr, RJ Lagow

文献索引：Baran Jr.; Lagow Journal of the American Chemical Society, 1990 , vol. 112, # 25 p. 9415 - 9416

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被引用次数: 24

摘要

The reactions werc quenched with dl-ethanol and analyzed by IH and 13C NMR on a GE GN-500 instrument and by GC/MS analysis on a Finnigan 4000 apparatus using a 30 m X 0.25 mm Heliflex bonded phase RSL-200 1. O-pm capillary column, with an injector temperature of 250 OC and an ionizer temperature of 150 OC. Percent deuterium incorporation was determined by mass spectroscopy.