The Coordination Chemistry of 1, 2??Bis [(diphenylphosphino) methyl] benzene with Nickel (II), Palladium (II), Platinum (II), and Platinum (0) and the X??Ray Crystals …
... Page 10. 2272 HELVETICA CHIMICA ACTA Vol. 73 (1990) from EtOH/Et,O. Yield 66%. Mp 205"(dec.) Anal. calc. ... Ligand 1 (1.91 g, 4.03 mmol) was then added and the suspension refluxed for another 20 min. It was then cooled and the solvent volume reduced to ca. 10 ml. ...
