A Practical Synthesis of trans-Dichlororuthenium ((S, S)-2, 6-Bis (4-isopropyl-2-oxazolin-2-yl)-pyridine)(ethylene) Amenable to Large-Scale Preparation

MJ Totleben, JS Prasad, JH Simpson…

文献索引：Journal of Organic Chemistry, , vol. 66, # 3 p. 1057 - 1060

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被引用次数: 33

摘要

... time (min) % CH3CN % H2O 0 30 70 10 30 70 20 70 30 30 70 30 35 30 70 40 30 70 Notes J. Org. Chem., Vol. 66, No. 3, 2001 1059 Page 4. the rich organic to approximately 25% of the starting volume (150 mL) at 40-50 °C under reduced pressure (15-20 inHg vacuum). ...