Total synthesis of (±)-cylindrospermopsin

C Xie, MTC Runnegar, BB Snider

文献索引：Matsumoto, Masakatsu; Ishida, Yasuko; Watanabe, Nobuko Heterocycles, 1985 , vol. 23, # 1 p. 165 - 170

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被引用次数: 46

摘要

... Volume: Page ... figure. Ozonolysis of 23 for 20 min cleaved the double bond, providing 72% of aldehyde 24 after reductive workup with Me 2 ... Eventually we found that slow addition of 1 equiv of cyanogen bromide 49 to 26 in dilute toluene solution gave the primary ...