... In this communication, we wish to report the desilylation of a wide range of silyl-protected primary ... ether (5S,6R)-methyl 5,6-bis(tert-butyldimethylsilyl-oxy)oct-7-enoate as a key synthetic intermediate.(20 ... to afford the corresponding diol in 97% yield after 10 min at 150 °C, entry 6a. ...
![Cyclohexene, 1-methyl-4-[1-methyl-1-[(trimethylsilyl)oxy]ethyl]结构式](https://image.chemsrc.com/caspic/154/90934-33-1.png)
![trimethyl[5-methyl-2-(1-methylethyl)cyclohexyloxy]silane结构式](https://image.chemsrc.com/caspic/435/62338-23-2.png)
![2-{[(tert-butyl)dimethylsilyl]oxy}-4-methyl-1-(1-methylethyl)cyclohexane结构式](https://image.chemsrc.com/caspic/009/129368-71-4.png)
