Organic & biomolecular chemistry

Continuous-flow, palladium-catalysed alkoxycarbonylation reactions using a prototype reactor in which it is possible to load gas and heat simultaneously

MA Mercadante, NE Leadbeater

文献索引：Mercadante, Michael A.; Leadbeater, Nicholas E. Organic and Biomolecular Chemistry, 2011 , vol. 9, # 19 p. 6575 - 6578

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被引用次数: 34

摘要

A prototype tube-in-tube reactor in which it is possible to load gas and heat simultaneously has been used in a continuous-flow approach to alkoxycarbonylation reactions of aryl iodides. In the stainless steel coil, liquid flows on the outside of a gas-permeable membrane. The coil can be heated and the temperature can be measured accurately via a probe touching the outer steel surface. A range of aryl iodides can be transformed to the ...