Continuous??Flow Microreactor Chemistry under High??Temperature/Pressure Conditions

T Razzaq, TN Glasnov…

文献索引：Razzaq, Tahseen; Glasnov, Toma N.; Kappe, C. Oliver European Journal of Organic Chemistry, 2009 , # 9 p. 1321 - 1325

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被引用次数: 89

摘要

Abstract High-temperature organic synthesis can be performed under continuous-flow conditions in a stainless steel microtubular flow reactor capable of achieving temperatures of 350 C and 200 bar. Under these extreme experimental environments transformations normally performed in a high-boiling solvent at reflux temperature–or under sealed-vessel microwave conditions–can be readily converted to a flow regime by using lower boiling ...