Chemosphere

Synthesis and mass spectrometry of some methoxylated PCB

Å Bergman, EK Wehler, H Kuroki, A Nilsson

文献索引：Bergman, A.; Klasson Wehler, E.; Kuroki, H.; Nilsson, A. Chemosphere, 1995 , vol. 30, # 10 p. 1921 - 1938

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被引用次数: 66

摘要

The syntheses of 46 methoxy-polychlorobiphenyls (MeO CBs), containing 3 to 7 chlorine atoms, are described. The MeO CBs were synthesized via the Cadogan diaryl coupling reaction of the appropriate polychloroaniline and polychloroanisole, or via the Ullmann coupling of a polychloroiodobenzene and 4-iodoanisole with subsequent chlorination of the isolated 4-MeO CB product. The synthesized MeO CBs were characterized by electron ...