Synthesis and properties of the vicinal trans dihydrodiols of anthracene, phenanthrene, and benzo [a] anthracene

RE Lehr, M Schaefer-Ridder…

文献索引：Lehr,R.E. et al. Journal of Organic Chemistry, 1977 , vol. 42, # 4 p. 736 - 744

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被引用次数: 91

摘要

736 J. Org. Chem., Vol. 42, No. 4, 1977 Lehr, Schaefer-Ridder, and Jerina 336," 45 ml of saturated KCl solution, and some solid KC1 were added. After stirring for 24 h at room temperature the benzene solu-tion was passed through a short column of alumina (to remove the Aliquat-336). After the usual workup there was obtained 3.0 g (90%) of 9: IR mp 175-176" C; m/e 366,368; NMR b 2.33 and 2.46 (s, 6 each, ArCH: J, 3.47 (s, 6, OCHR), ...