Practical Asymmetric Synthesis of an Edivoxetine· HCl Intermediate via an Efficient Diazotization Process

ME Kopach, PC Heath, RB Scherer…

文献索引：Buckley, Benjamin R.; Patel, Anish P.; Wijayantha Journal of Organic Chemistry, 2013 , vol. 78, # 3 p. 1289 - 1292

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被引用次数: 2

摘要

... Select a Journal or Book ... Although up to an 8% yield of the undesired R enantiomer could be rejected in the downstream crystallization of 1, it was ... After the n-heptane extraction, a solution of p-TsOH monohydrate (2 equiv) in deionized water (1 volume) was added to the ...