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Synthesis and crystal structure of the dimer bis {[bis (trimethylsilylmethyl) arsino] diphenylgallane}

RL Wells, AP Purdy, AT McPhail, CG Pitt

文献索引:Wells, Richard L.; Purdy, Andrew P.; McPhail, Andrew T.; Pitt, Colin G. Journal of Organometallic Chemistry, 1986 , vol. 308, p. 281 - 288

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被引用次数: 1

摘要

Abstract The dimer [(Me 3 SiCH 2) 2 AsGaPh 2] 2, obtained from the reaction of (Me 3 SiCH 2) 2 AsH with Ph 3 Ga, has been characterized by partial elemental analysis, NMR spectroscopy, cryoscopic molecular weight determination, and complete single-crystal X-ray analysis. Crystals of the dimer are triclinic, space group P Full-size image (< 1 K)