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Existence and reactivity of bicyclic annulenones. 2. Bicyclo [3.3. 0] octa-1 (5), 3, 7-triene-2, 6-dione

F Gavina, AM Costero, AM Gonzalez…

文献索引:Gavina, Francisco; Costero, Ana M.; Gonzales, Ana M.; Luis, Santiago V. Journal of Organic Chemistry, 1987 , vol. 52, # 14 p. 2997 - 2999

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被引用次数: 8

摘要

Gas chromatography was performed with a Delsi IGC 120 FL Model, the column used was 3% SP 2100 on 120-140 mesh, Chromosorb G, 1.50 m. Liquid chromatography was performed on silica gel 60 (Merck, 0.063-0.200 mm) on a 15 X 150 mm column. PE and TBAB (Fluka) D, L-threitol (Aldrich), and a-methyl glucoside (Janssen) were dried before use (60" C under reduced pressure).