Convenient synthesis of symmetrical diketosulfides from enolizable ketones using [hydroxy (tosyloxy) iodo] benzene and na2S⋅ 9H2O

NN Karade, GB Tiwari, SV Gampawar…

文献索引：Karade, Nandkishor N.; Tiwari, Girdharilal B.; Gampawar, Sumit V.; Shinde, Sandeep V. Heteroatom Chemistry, 2009 , vol. 20, # 3 p. 172 - 176

全文：HTML全文

被引用次数: 5

摘要

Abstract An efficient method for the preparation of symmetrical diketosulfides of the type ArCOCH 2 SCH 2 COAr has been developed from the reaction of [hydroxy (tosyloxy) iodo] benzene with various acetophenones, followed by treatment with Na 2 S⋅ 9H 2 O.© 2009 Wiley Periodicals, Inc. Heteroatom Chem 20: 172–176, 2009; Published online in Wiley InterScience (www. interscience. wiley. com). DOI 10.1002/hc. 20524