Ozonolysis of vinyl fluoride: identification of ozonides and doubly fluorinated products

U Mazur, RP Lattimer, A Lopata…

Index: Mazur,U. et al. Journal of Organic Chemistry, 1979 , vol. 44, p. 3181 - 3185

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Citation Number: 10

Abstract

Results The ozonolyses of C2H3F were conducted at low temperature either in methyl chloride or in isobutane or neat, using standard techniquesQ as described in the Experimental Section. A workup procedure involving distillation of the crude reaction mixture through traps held at-63,-95, and-196" C and subsequent VPC and spectroscopic analysis of each trap was devised. The coldest trap was found to contain HCOF, C2H3F, and ( ...