e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Bulletin des Sociétés Chimiques Belges

Identification D'isomères du Dodécane Mesures des Indices de Rétention a Plusieurs Températures

M De Laet, B Tilquin

Index: Laet, M. de; Tilquin, B. Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 4 p. 345 - 355

Full Text: HTML

Citation Number: 1

Abstract

Abstract Pure 3-methylpentane was irradiated in its solid vitreous state at 77 K. The qualitative analysis of the dimeric products was made by mean of capillary chromatography coupled with mass spectrometry. The identification of the dimers, highly branched dodecanes, required the synthesis of compounds whose structure was defined by NMR 13 C DEPT; they were characterised by their retention index measured at several ...

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4-diethyl-3,4-dimethylhexane Structure

3,4-diethyl-3,4...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3-ethyl-3,6-dimethyloctane Structure

3-ethyl-3,6-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3,5-diethyl-3-methylheptane Structure

3,5-diethyl-3-m...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

1-Pentene, 3-methyl- Structure

1-Pentene, 3-methyl-

~72%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4-diethyl-3,4-dimethylhexane Structure

3,4-diethyl-3,4...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3-ethyl-3,6-dimethyloctane Structure

3-ethyl-3,6-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3,5-diethyl-3-methylheptane Structure

3,5-diethyl-3-m...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3-ethyl-3,6-dimethyloctane Structure

3-ethyl-3,6-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4-diethyl-3,4-dimethylhexane Structure

3,4-diethyl-3,4...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3-ethyl-3,6-dimethyloctane Structure

3-ethyl-3,6-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3,5-diethyl-3-methylheptane Structure

3,5-diethyl-3-m...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

1-Pentene, 3-methyl- Structure

1-Pentene, 3-methyl-

~0%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

1-Pentene, 3-methyl- Structure

1-Pentene, 3-methyl-

~0%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,5,6-tetramethyloctane Structure

3,4,5,6-tetrame...

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

6-ethyl-3,4-dimethyloctane Structure

6-ethyl-3,4-dim...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,6-diethyloctane Structure

3,6-diethyloctane

3,4,7-trimethylnonane Structure

3,4,7-trimethyl...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3,4-diethyl-3,4-dimethylhexane Structure

3,4-diethyl-3,4...

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

Detail

Pentane, 3-methyl- Structure

Pentane, 3-methyl-

~%

DECANE,3,8-DIMETHYL- Structure

DECANE,3,8-DIMETHYL-

3-ethyl-3,4,5-trimethylheptane Structure

3-ethyl-3,4,5-t...

3,5-diethyl-3-methylheptane Structure

3,5-diethyl-3-m...

Detail