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e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521

Helvetica chimica acta

Synthesis of Indole Derivatives by [2+ 2] Photocycloaddition of Indoline??2??thiones with alkenes and photodesulfurization of indoline??2??thiones

T Nishio, M Oka

Index: Helvetica Chimica Acta, , vol. 80, # 2 p. 388 - 397

Full Text: HTML

Citation Number: 14

Abstract

... 2.3. yH Abstraction Reaction of I-Acylindoline-2-thiones 11-p and Their 0x0 Ana- logues 2 ad. As described briefly in Sect. 2.1, irradiation of l-acylindoline-2-thiones Page 5. 392 HELVETICA CHIMICA ACTA - Vol. 80 (1997) Scheme 4 xyy7J +xmR' N 'mS ...

 Related Synthetic Route
1-benzylindoline-2-thione Structure

104501-75-9

1-benzylindolin...

~12%

1-benzyl-3-ethyl-1H-indole Structure

17017-59-3

1-benzyl-3-ethy...

1-benzylindole Structure

3377-71-7

1-benzylindole

Learn More
1-benzylindoline-2-thione Structure

104501-75-9

1-benzylindolin...

Triethylamine Structure

121-44-8

Triethylamine

~12%

1-benzyl-3-ethyl-1H-indole Structure

17017-59-3

1-benzyl-3-ethy...

1-benzylindole Structure

3377-71-7

1-benzylindole

Learn More
1-acetyl-3,3-dimethylindolin-2-one Structure

72934-84-0

1-acetyl-3,3-di...

Ethanol Structure

64-17-5

Ethanol

~94%

3,3-Dimethylindolin-2-one Structure

19155-24-9

3,3-Dimethylind...

ethyl acetate Structure

141-78-6

ethyl acetate

Learn More
2H-Indole-2-thione,1,3-dihydro-1-phenyl Structure

73425-20-4

2H-Indole-2-thi...

Triethylamine Structure

121-44-8

Triethylamine

~34%

phenylindole Structure

16096-33-6

phenylindole

3-ethyl-1-phenyl-1H-indole Structure

112817-89-7

3-ethyl-1-pheny...

Learn More
1-METHYL-1,3-DIHYDRO-INDOLE-2-THIONE Structure

13637-38-2

1-METHYL-1,3-DI...

~11%

1-Methylindole Structure

603-76-9

1-Methylindole

1-methyl-3--ethyl indole Structure

45999-11-9

1-methyl-3--eth...

Learn More
1-acetyl-3,3-dimethylindolin-2-one Structure

72934-84-0

1-acetyl-3,3-di...

Ethanol Structure

64-17-5

Ethanol

~94%

3,3-Dimethylindolin-2-one Structure

19155-24-9

3,3-Dimethylind...

ethyl acetate Structure

141-78-6

ethyl acetate

Learn More
Ethanol Structure

64-17-5

Ethanol

N/A Structure

189623-31-2

N/A

~95%

3,3-diphenyl-1H-indol-2-one Structure

1922-79-8

3,3-diphenyl-1H...

ethyl acetate Structure

141-78-6

ethyl acetate

Learn More
1-METHYL-1,3-DIHYDRO-INDOLE-2-THIONE Structure

13637-38-2

1-METHYL-1,3-DI...

Triethylamine Structure

121-44-8

Triethylamine

~11%

1-Methylindole Structure

603-76-9

1-Methylindole

1-methyl-3--ethyl indole Structure

45999-11-9

1-methyl-3--eth...

Learn More
Related Articles: More...
N-alkylation of pyrrole, indole, and several other nitrogen ...

[Sukata, Kazuaki Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 1 p. 280 - 284]
DABCO-and DBU-accelerated green chemistry for N-, O-, and S-...

[Shieh, Wen-Chung; Lozanov, Mario; Loo, Mauricio; Repic, Oljan; Blacklock, Thomas J. Tetrahedron Letters, 2003 , vol. 44, # 24 p. 4563 - 4565]
Palladium catalyzed N-alkylation of amines with alcohols

[Zhang, Yan; Qi, Xiujuan; Cui, Xinjiang; Shi, Feng; Deng, Youquan Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1334 - 1338]
Palladium catalyzed N-alkylation of amines with alcohols

[Zhang, Yan; Qi, Xiujuan; Cui, Xinjiang; Shi, Feng; Deng, Youquan Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1334 - 1338]
General and efficient synthesis of 2, 3-unsubstituted indole...

[Sun, Nan; Hong, Lingfen; Huang, Fang; Ren, Hong; Mo, Weimin; Hu, Baoxiang; Shen, Zhenlu; Hu, Xinquan Tetrahedron, 2013 , vol. 69, # 19 p. 3927 - 3933]

Detail Synthetic Route


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