Organometallics

Synthesis and Structure of a Tetrahydroxydisilane and a Trihydroxycyclotrisiloxane with All the OH Functions in cis Position

C Ackerhans, HW Roesky, T Labahn, J Magull

Index: Graalmann, Onno; Klingebiel, Uwe; Clegg, William; Haase, Martin; Sheldrick, George M. Chemische Berichte, 1984 , vol. 117, # 9 p. 2988 - 2997

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Citation Number: 20

Abstract

... empirical formula, 2 C 14 H 42 O 4 Si 6 ·CH 3 OH· 1 / 4 C 6 H 6, C 21 H 60 O 6 Si 9. ... cell volume [Å 3 ], 2768.6(5), 1933.7(5 ... δ −7.4 (Si(OH) 2 ), −0.6 (SiMe 3 ). IR (KBr, Nujol): ν̃ 3631, 3348, 1301, 1251, 1062, 1025, 1007, 857, 845, 777, 723, 681, 551, 429 cm - 1 . MS (EI): m/e (%) 393 ...