CHSH), 3.17 (s, I, OH), 3.25 (m, 1,-CHSH), and 4.12 ppm (A portion of AMNX, 1, J,.,,, a. endo= 10 Hz, J,,,,. 3. exo= 4.5 Hz, J2. eno6. exo= 2.1 Hz,-CHOH). Addition of F~ CCOZH causes the signal at 3.25 to shift to 3.47 ppm (* 15&, 6. exo= 10.5 Hz, J5. exo= 5.7 Hz, JP. exo, e. oxo= 2.5 He) and the signal at 4.12 to shift to 4.37 ppm (J,. ero3. endo= 10.0, JP. exo, 3. exo= 5.0 Hz, and JZ-exo6. exo= 2.5 Ha); mass spectrum (70 eV) m/e (re1 intensity) 186 ...
[Kotkar, Dilip; Mahajan, Satish W.; Mandal, Arun K.; Ghosh, Pushpito K. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1749 - 1752]
[Kotkar, Dilip; Mahajan, Satish W.; Mandal, Arun K.; Ghosh, Pushpito K. Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1749 - 1752]
