... 1, Academic Press, New York, NY, 1965, pp 3-51; (b) Y. Wolman in "The Chemistry of the Amino Group," S. Patai, Ed., Intersoience, Kew ... The resulting clear solution was stirred at room tem- perature for 2 hr and poured into 200 ml of HzO, and the organic layer was ... 3408 J . Org. ...