Tetrahedron Letters

Hypervalent iodine in organic synthesis: Acetal formation under basic conditions and carbon deuteriation of the aldehydo group

RM Moriarty, H Hu

Index: Moriarty, Robert M.; Hu, Henry Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1537 - 1540

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Citation Number: 4

Abstract

Abstract Aldazines upon treatment with phenyliodosyl diacetate in CH 3 OH or CH 3 OD and NaOCH 3 are converted smoothly into two equivalents of the corresponding aldehyde dimethylacetal with deuterium incorporation at the aldehydic carbon atom in the case of CH