Carbohydrate Research

Isolation and identification of products in the reaction of 2-acetamido-3, 4, 6-tri-O-acetyl-1, 5-anhydro-2-deoxy-d-arabino-hex-1-enitol with theophylline

N Pravdić, B Danilov

Index: Pravdic, Nevenka; Danilov, Boris Carbohydrate Research, 1981 , vol. 97, p. 31 - 44

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Citation Number: 3

Abstract

Abstract Fusion of 2-acetamido-3, 4, 6-tri-O-acetyl-1, 5-anhydro-2-deoxy-d-arabino-hex-1- enitol with theophylline, in the presence of boron trifluoride etherate as the catalyst, caused condensation to occur. This reaction afforded a variety of products of nucleosidic character, which were successively separated by repeated chromatography on silica gel. The structures of the products were determined, on the basis of X-ray crystallographic analysis ...