Synthesis and properties of cobalt (III) complexes of 4-substituted pyridine-capped dioxocyclams

AL Reiff, EM Garcia-Frutos, JM Gil…

Index: Przystas, Theodore J.; Fife, Thomas H. Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 3 p. 393 - 399

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Citation Number: 10

Abstract

... Select a Journal or Book ... white solid with EtOAc/hexane (10 mL/10 mL) and drying under vacuum afforded the desired 4-(N,N-dimethylamino)phenylboronic acid (2.84 g, 17.2 mmol): yield 86%; 1 H NMR (CDCl 3 , 300 MHz) δ 8.11 (d, J = 8.7 Hz, 2H), 6.81 (d, J = 8.1 Hz ...