Journal of the American Chemical Society

The Preparation of Aldehydes, Ketones, and Acids by Ozone Oxidation

AL Henne, P Hill

Index: Henne; Hill Journal of the American Chemical Society, 1943 , vol. 65, p. 753

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Citation Number: 36

Abstract

Naphthy1carbamate.-Four grams of 2, 3, 4, 5, 6-0-pentamethyl-(levo)-sorbitol was added to 3.5 g. of a-naphthyl isocyanate, shaken well and allowed to stand overnight. The general procedure used was that described by Bickel and French.''Crystals of the by-product, di-a- naphthyl urea, separated and the reaction solution set to a semisolid inass. Petroleum ether was added (bp 60-110) and the mixture boiled and filtered rapidly in order to remove the ...

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