The Journal of organic chemistry

Improved synthesis of aryltriethoxysilanes via palladium (0)-catalyzed silylation of aryl iodides and bromides with triethoxysilane

AS Manoso, P DeShong

Index: Rossi, Renzo; Carpita, Adriano; Messeri, Tommaso Gazzetta Chimica Italiana, 1992 , vol. 122, # 1 p. 65 - 72

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Citation Number: 96

Abstract

... Volume: Page: Digital Object Identifier (DOI). ... a Reactions of 4-bromoanisole (1) (1.0 mmol) with HSi(OEt) 3 (1.5 mmol) were performed at room temperature for 12h in 4 mL of solvent by using Pd(dba) 2 (5 mol %), phosphine (10 mol %), and base (3 mmol). ...