Oxidation of Alcohols to Carbonyl Compounds with Diisopropyl Azodicarboxylate Catalyzed by Nitroxyl Radicals

M Hayashi, M Shibuya, Y Iwabuchi

Index: Journal of Organic Chemistry, , vol. 77, # 6 p. 3005 - 3009

Full Text: HTML

Citation Number: 32

Abstract

... The Journal of Organic ... 2 (0.65 mL) was refluxed with stirring for 8 h. Saturated NaHCO 3 (2 mL) was added and extracted with CH 2 Cl 2 . The organic layer was ... δ 9.74 (d, J = 1.5 Hz, 1H), 7.30–7.15 (m, 5H), 2.65 (t, J = 7.7 Hz, 2H), 2.43 (dt, J = 7.2, 1.5 Hz, 2H), 1.95 (tt, J = 7.7, 7.2 ...