Tetrahedron

An efficient synthesis of 1α, 25-dihydroxy vitamin D 3

L Vanmaele, PJ De Clercq, M Vandewalle

Index: Tetrahedron, , vol. 41, # 1 p. 141 - 144

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Citation Number: 29

Abstract

Terrakhv~ Vol. ... mmol), imidazole (295 mg; 4.35 mmol) and $e&-bu- tyldimethylsilyl chloride (367 mg; 2.44 mmol) in DMF (20 mL) is stirred under argon at 25OC for 5 h. After addition of an equal volume of hexane ... LJ Vanmaele, PJ De Clercq and M. Vandewalle, Tetrahedron Lett ...