Studies on the synthesis of 1-azaspiro [5.5] undecanes related to histrionicotoxin

JJ Venit, M DiPierro, P Magnus

Index: Journal of Organic Chemistry, , vol. 54, # 18 p. 4298 - 4301

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Citation Number: 19

Abstract

... 2) For a comprehensive review of work before 1985, see: Daly, JW Progress in the Chemistry of Natural ... 4300 J. Org ... The organic layer was separated, dried (Na2S04), and evaporated in vacuo to give 9/10 (1:l) (0.38 g, 74%), which was directly acetylated with acetic anhydride (3 ...