Catalytic hydrolysis of phosphate esters in microemulsions. 3. Analysis of the hydrolysis products of p-nitrophenyl diphenyl phosphate via 31P NMR

BA Burnside, LL Szafraniec, BL Knier…

Index: Burnside, Beth A.; Szafraniec, Linda L.; Knier, Barry L.; Durst, H. Dupont; Mackay, Raymond A.; Longo, F.R. Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 2009 - 2011

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Citation Number: 22

Abstract

Results An Examination of Authentic Samples. Microemulsions containing authentic samples of various phosphate esters suspected as products were prepared according to the procedure above, to give a final concentration of 4 mg/mL in the microemulsions. The resonance line positions for these compounds are shown in Table 11. We also observe additional peaks due to phosphate species in the spectra at-5.5 ppm,-4.2 ppm, and+ 1.0 ...