The Synthesis of Certain 5-Deoxy-D-ribofuranosylpurines1

HM Kissman, BR Baker

Index: Kissman; Baker Journal of the American Chemical Society, 1957 , vol. 79, p. 5534,5537

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Citation Number: 53

Abstract

1, 2, 3-Tri-0-acetyl-5-deoxy-~-ribofuranose (11), obtained in three steps from methyl 2, 3-0- isopropylidene-5-~-mesy~-D-ribofuranoside (IV), was converted to the 1-chloro sugar (I). Condensation of I with chloromercuri-6-dimethylamin0-purine, followed by deblocking, aff ordcd 6-dimetliylamino-0-(~-deoxy-~-~-r~ bofuranosyl)-purine(VII). Condensation of I with chloromercuri-6-benzamidopurine afforded, after deblocking, 5'-deosyadenosine (VIII) ...

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