Journal of Chemical Crystallography

Self-Assembly of N-1, 3-Dithiolan-2-ylidene-N′-[1-furan-2-yl-meth-(E)-ylidene]-hydrazine via Left-Handed Helical Chains of S··· O Short Contacts and C–H··· N Inter- …

YH Liu, ZG Li, LJ Yang, XL Liu

Index: Liu, Yong-Hong; Li, Zhi-Gang; Yang, Ling-Juan; Liu, Xiao-Lan Journal of Chemical Crystallography, 2008 , vol. 38, # 11 p. 867 - 871

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Citation Number: 3

Abstract

Abstract The title compound, N-1, 3-Dithiolan-2-ylidene-N′-[1-furan-2-yl-meth-(E)-ylidene]- hydrazine was synthesized via furfural with 2-hydrazono-1, 3-dithiolane and characterized by elemental analysis, 1 H NMR, 13 C NMR, IR, UV–Vis and single crystal XRD. The crystal belongs to orthorhombic, space group F2 1 2 1 2 1 with unit cell parameters a= 6.4035 (9) Å, b= 11.8835 (16) Å, c= 12.3809 (17) Å, V= 942.1 (2) Å 3, Z= 4, Dc= 1.497, Mr= 212.28, μ= ...