Synthesis

Efficient method for selective cleavage of acetals and ketals using peroxymonosulfate on alumina under solvent-free conditions

DS Bose, B Jayalakshmi, AV Narsaiah

Index: Bose, D. Subhas; Jayalakshmi; Narsaiah, A. Venkat Synthesis, 2000 , # 1 p. 67 - 68

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Citation Number: 18

Abstract

Abstract: In an environmentally benign solvent-free system, acetals and ketals are rapidly cleaved with peroxymonosulfate-alumina under microwave irradiation in high yields. Key words: peroxymonosulfate, acetals, alumina, ketals, solid support, hydrolysis, protecting groups, microwaves, solvent-free conditions