m-Chloroperoxybenzoic acid oxidation of S-phenyl 2, 2-dimethylpropanethiosulfinate

F Freeman, CN Angeletakis…

Index: Freeman, Fillmore; Angeletakis, Christos N.; Maricich, Tom J. Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3403 - 3408

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Citation Number: 14

Abstract

Results The 1 equiv MCPBA oxidation of 18 was performed at-30" C in CDC13 under a nitrogen atmosphere for 1 h. The product mixture was filtered in an inert atmosphere at-45" C as quickly as possible in order to remove m-chlorobenzoic acid (MCBA). The'H NMR and 13C NMR spectra of the filtrate were recorded as soon as possible after filtration.